novel synthesis of pyrimido[4,5- e] [1,3,4] thiadiazines as potential 15- lipoxygenase inhibitors

نویسندگان

abdolhassan doulah

department of nursing, faculty of nursing and midwifery, islamic azad university, ahvaz branch, ahvaz 6134968875, iran masoud mirzaei

department of chemistry, school of sciences, ferdowsi university of mashhad, mashhad, 91775-1436, iran mohsen nikpour

department of chemistry, school of sciences, islamic azad university, ahvaz branch, ahvaz, 6134968875, iran yaghoub farbood

physiology research center and department physiology, medicine faculty, ahwaz jondishapour university of medical sciences, ahwaz, iran

چکیده

treatment of 1-(5-bromo-2-chloro-6-methylpyrimidin-4-yl)-1-methylhydrazine withdimethylthiocarbamoylchloride gave 7-chloro-n,n, 1,5-tetramethyl-1h-pyrimido[4,5-e][1,3,4]thiadiazin-3-amine in basic acetonitrile. the latter compounds were reacted withsecondary amines in boiling ethanol to afford the related 7-amino derivatives.

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منابع مشابه

Novel synthesis of Pyrimido[4,5- e] [1,3,4] thiadiazines as potential 15- lipoxygenase inhibitors

Treatment of 1-(5-bromo-2-chloro-6-methylpyrimidin-4-yl)-1-methylhydrazine withdimethylthiocarbamoylchloride gave 7-chloro-N,N, 1,5-tetramethyl-1H-pyrimido[4,5-e][1,3,4]thiadiazin-3-amine in basic acetonitrile. The latter compounds were reacted withsecondary amines in boiling ethanol to afford the related 7-amino derivatives.

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Design and synthesis of new esters of terpenoid alcohols as 15-lipoxygenase inhibitors

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Design, synthesis, and SAR study of isopropoxy allylbenzene derivatives as 15-lipoxygenase inhibitors

Objective(s): Allylbenzenes have been recently developed as inhibitors of lipoxygenases. They decrease peroxidation activity via mimicking 1,4-unsaturated bonds of fatty acids by their allyl portion. We designed and synthesized new derivatives of allyl benzenes (6a-f) with isopropoxy and amide substituents at ortho and meta positions towards allyl group, respectively. ...

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Novel synthesis of Pyrimido[4,5- e] [1,3,4] thiadiazines

Treatment of 1-(5-bromo-2-chloro-6-methylpyrimidin-4-yl)-1-methylhydrazine with dimethylthiocarbamoylchloride gave 7-chloro-N,N,1,5-tetramethyl-1H-pyrimido[4,5-e][1,3,4]thiadiazin-3-amine in basic acetonitrile. The latter compounds were reacted with secondary amines in boiling ethanol to afford the related 7-amino derivatives.

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Novel synthesis of Pyrimido[4,5- e] [1,3,4] thiadiazines

Treatment of 1-(5-bromo-2-chloro-6-methylpyrimidin-4-yl)-1-methylhydrazine with dimethylthiocarbamoylchloride gave 7-chloro-N,N,1,5-tetramethyl-1H-pyrimido[4,5-e][1,3,4]thiadiazin-3-amine in basic acetonitrile. The latter compounds were reacted with secondary amines in boiling ethanol to afford the related 7-amino derivatives.

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New Insight into the SAR of Pyrimido [4,5-b][1,4] Benzothiazines as 15-lipoxygenase Inhibitors

  Objective(s): Recently we reported that the soybean 15-lipoxygenase (SLO) inhibitory activity of pyrimido[4,5-b][l,4]benzothiazines largely depends on the orientation of sulfur atom of thiazine core towards FeIII-OH in the active site pocket of the enzyme with subsequent oxidation of sulfur to sulfoxide. In this paper the results of a comparative study on the SLO inhibitory activities of the ...

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عنوان ژورنال:
journal of the iranian chemical research

جلد ۴، شماره ۲، صفحات ۹۳-۹۶

کلمات کلیدی
[ 1 , ' ( 5 ' , ' b r o m o ' , 2 , ' c h l o r o ' , 6 , ' m e t h y l p y r i m i d i n ' , 4 , ' y l ) ' , 1 , ' m e t h y l h y d r a z i n e ' , ' d i m e t h y l t h i o r c a r b a m o y l c h l o r i d e ' , ' p y r i m i d o t h i a d i a z i n e ' , ' c y c l o c o n d e n s a t i o n ' ]

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